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Agilent 6130B Single Quadrupole Mass Spec w/ Agilent 1200 MS/LC System
Maximum Scan Speed
10,400 Da/sec
Polarity Switching
30 msec
Mass Range
10 - 3,000 m/z
- Single-point data system method capability with full control of Agilent 1200 Series LC Systems and 6100 Series Single Quadrupole LC/MS Systems
- Wide range of ionization sources of Electrospray (ESI), Multimode source (simultaneous ESI and APCI), Atmospheric pressure chemical ionization (APCI), ChipCube for integrated nanoLC, and Atmospheric pressure photoionization (APPI).
- Detector Types of high energy conversion dynode and high gain electron multiplier horn.
- Features turbo-molecular vacuum pump with one mechanical pump.
- Achieves specifications with autotune for mass range 10–3,000 m/z.
The Agilent 6130B Single Quadrupole Mass Spec w/ Agilent 1200 MS/LC System delivers unmatched analytical performance and proven day-after-day reliability from routine QC to research applications. This 6130B model is specifically a flexible, high performance solution ideal for any quantitation application with 3000 Da mass range and 1 pg sensitivity. This system allows users to rapidly screen compounds and confirm molecular weights, purify target compounds in complex mixtures, quantitate target compounds, positively identify impurities and more. The Agilent 6130B Single Quadrupole Mass Spec provides unmatched sensitivity, simplifying sample preparation and LC method development. An ultrafast scan speed allows users to take full advantage of UHPLC separations, as well as featuring ultrafast ion polarity switching to return maximum information from a single injection, even with narrow LC peaks. The Agilent 6130B Single Quadrupole Mass Spec w/ Agilent 1200 MS/LC System can be fully controlled from the included Agilent ChemStation Workstation Software, which allows for user-friendly operation in data acquisition, analysis, instrument control, automation, and more.
This Agilent system is in excellent condition and will be fully tested to perform at factory
specifications before being shipped.
The Agilent 6130B Single Quadrupole Mass Spec w/ Agilent 1200 MS/LC System includes:
- > Agilent 6130B Single Quadrupole Mass Spec
- > Agilent Rotary Vane Vacuum Pump
- > G1948B ESI Ionization Source
- > G1312A Binary Pump
- > G1329A Autosampler
- > G1330B ALS Thermostat
- > G1316B TCC
- > G1379B Degasser
- > G1315B DAD Detector
- > Windows 10 Professional 64-Bit Data Station with Flatscreen Monitor
- > ChemStation Version 4.3 Software Installed
- > All Power Cords
- > Can/Crossover Cables
- > Agilent Lan Interface Card Built-In
- > Solvent Tubing
- > Capillaries
- > Agilent 4 Peak Test w/ Lab Advisor Diagnostics Report & Mass Spec Tuning Report
- > Full 180 Day Parts and Labor Warranty
Below is a List of Diagnostic Tests Performed On This System
- Filter Test: The test moves the filter into the light path and measures the relative absorbance in the filter position.
- Dark Current Test: The test measures the dark current from the detector optic.
- Holmium Oxide Test: The test measures the Holmium spectrum from the built-in Holmium filter. The spectrum is evaluated for peaks at different wavelengths.
- Lamp Intensity Test: The test verifies functionality of the UV lamp at various wavelengths.
- Wavelength Intensity Test: The test confirms the accuracy of wavelengths measured.
- Baseline Noise Test: The test measures the amount of baseline noise drift identified by the detector.
- Pressure Test: The pressure test is a quick, built-in test designed to demonstrate the pressure tightness (up to 400 bar) of the system.
- Leak Test: The leak test is a built-in troubleshooting designed to demonstrate the leak-tightness of the pump.
- Thermostat Test: Evaluates the cooling and heating performance of the two Peltier elements.
- Injector Steps: Performs each movement of the sampling sequence under manual control. This is useful for confirming autosampler functionality.
- 4 Peak Test (Isocratic Standard): Standard test published by Agilent to confirm complete functionality of the 1200 HPLC System.
Agilent 6130B Single Quadrupole Mass Spec Specifications
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Maximum Scan Speed
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10,400 Da/sec
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SIM Sensitivity, ESI Positive
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Signal-to-noise ratio > 250:1 (1 pg of reserpine injected on column,
quantifying the m/z 609 ion)
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SIM Sensitivity, APCI Positive
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Signal-to-noise ratio > 100:1 (1 pg of reserpine injected on column,
quantifying the m/z 609 ion)
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Polarity Switching
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30 msec (switching time from positive to negative polarity)
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Mass Resolution (Autotune)
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Unit resolution (full width at half maximum)
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Mass Stability
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< 0.1 amu or 100 ppm, whichever is larger (over 12 hours)
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Mass Accuracy
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± 0.13 Da
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Maximum SIM Dwell Time
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5 msec
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Maximum SIM Transitions
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100 (one time segment)
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Dynamic Range
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> 6 × 10^6
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Mass Range
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10–3,000 m/z
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Single Point of Control
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Single-point data system method capability with full control of Agilent 1200 Series LC Systems and 6100 Series Single Quadrupole LC/MS Systems
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Time Programming
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SIM ion selections, Scan functions, Fragmentor voltage, External CAN valves
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Ionization Sources
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Electrospray (ESI), Multimode source (simultaneous ESI and APCI), Atmospheric pressure chemical ionization (APCI), ChipCube for intergrated nanoLC, Atmospheric pressure photoionization (APPI)
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Detector
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High energy conversion dynode and high gain electron multiplier horn
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Vacuum System
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One turbo-molecular pump with one mechanical pump
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Dimensions (W x H x D)
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14 x 18 x 25 in. (35 x 45 x 63.5 cm)
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Weight
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137.6 lb. (63.4 kg.)
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Electrical Requirements
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200-230VAC, 60Hz or 200-240VAC, 50Hz
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Click Here to View Specifications for the Agilent 1200 MS/LC System
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DAD Detector
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Specification
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Detection Type
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1024-element photodiode array
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Light Source
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Deuterium and tungsten lamps
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Wavelength Range
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190 - 950 nm
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Short Term Noise (ASTM) Single and Multi-Wavelength
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± 1 × 10^-5 AU at 254 and 750 nm
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Drift
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2 × 10^-3 AU/hr at 254 nm
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Linear Absorbance Range
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> 2.0 AU (upper limit)
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Wavelength Accuracy
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± 1 nm
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Wavelength Bunching
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1 - 400 nm
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Slit Width
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1, 2, 4, 8, 16 nm
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Diode Width
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< 1 nm
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Flow Cells
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Standard: 13 µL volume, 10 mm cell path length and 120 bar (1740 psi) pressure maximum
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Binary Pump
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Specification
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Hydraulic System
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Two dual piston in series pumps with proprietary servo-controlled variable stroke drive, floating piston design and active inlet valve
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Setable Flow Range
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0.001 – 5 ml/min, in 0.001 ml/min increments
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Flow Range
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0.1 - 5.0 mL/min
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Flow Precision
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< 0.07% RSD or < 0.02 min SD, whatever is greater
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Flow Accuracy
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± 1% or 10 µl/min, what ever is greater
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Pressure Operating Range
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Operating range 0 400 bar (0 – 5880 psi) up to 5 ml/min
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Pressure Pulsation
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< 2 % amplitude (typically < 1 %), at 1 ml/min isopropanol, at all pressures > 1 MPa
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Compressibility Compensation
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User-selectable, based on mobile phase compressibility
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Recommended pH Range
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1.0 - 12.5, solvents with pH < 2.3 should not contain acids which attack stainless steel
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Gradient Formation
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High-pressure binary mixing
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Delay Volume
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800 – 1100 µl, dependent on back pressure
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Autosampler
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Specification
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Injection Range
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0.1 - 100 µl in 0.1 µl increments
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Precision
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Typically < 0.25 % RSD of peak areas from 5 to 100 µl
Typically < 1 % RSD of peak areas from 1 to 5 µl
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Pressure Range
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Operating range 0 - 60 MPa (0 - 600 bar, 0 - 8850 psi)
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Sample Viscosity Range
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0.2 – 50 cp
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Sample Capacity
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100 × 2 mL vials in 1 tray
40 × 2 mL vials in ½ tray
15 × 6 mL vials in ½ tray (Agilent vials only)
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Injection Cycle Time
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50 s for draw speed 200 µL/min, ejection speed 200 µL/min, injection volume 5 µL
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Carryover
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Typically < 0.1 %, < 0.05 % with external needle cleaning
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ALS Thermostat
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Specification
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Temperature Range
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4°C to 40°C in 1°C increments
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Temperature Accuracy at Ambient Temperatures < 25°C and Humidity < 50%
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-1°C to +4°C at a setpoint of 4°C
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Temperature Accuracy at Ambient Temperatures > 30°C and Humidity > 60%
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-1°C to +5°C at a setpoint of 4°C
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Column Compartment
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Specification
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Temperature Range
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Ambient -10°C to 100°C at flow rates up to 2.5 mL/min
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Temperature Stability
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± 0.05 °C
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Temperature Accuracy
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± 0.8°C
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Warm-Up/Cool-Down Time
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5 minutes from ambient to 40°C
10 minutes from 40°C to 20°C
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Degasser
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Specification
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Number of Solvent Channels
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4
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Flow Range
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0 - 5 mL/min per channel
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Internal Volume Per Channel
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Typically 1 ml per channel
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Materials in Contact with Solvent
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PTFE, FEP,PEEK
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pH Range
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1 - 14
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Computer Specifications
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Model
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Dell Optiplex 7010 Desktop PC
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Processor
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Intel Core i5-6500 Processor 3.2GHz
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RAM
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16GB
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Hard Drive
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250GB Internal SSD
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Operating System
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Windows 10 Professional, 64bit
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